产品分类
YMC*GEL(HG) / YMC-Omega填料
制备填料YMC*GEL系列由正相色谱填料与反相色谱填料两种模式产品组成。该系列产品有丰富的官能团种类与填料粒径可供选择。YMC*GEL HG系列采用高密度、高强度的硅胶为基质,即使是反复进行填料的装填与卸载都基本无填料破损,因此可以供客户长期使用。高性能的YMC*GEL/YMC*GEL HG填料具有高性价比的特点,在国内外得到了广泛使用。
要点
- 各种官能团、颗粒径产品系列
- 采用高密度高机械强度的硅胶基质(YMC*GEL HG)
- 非常适于HPLC用动态轴向压缩柱的大量纯化制备
- 快速层析色谱、开放型色谱填料系列
产品特点
| 优秀的机械强度(YMC*GEL HG)
YMC*GEL HG系列采用了高密度硅胶,因此具有高机械强度。使用动态轴向压缩柱即使进行10次以上的反复装填,也未发现填料颗粒的破损及柱压的升高。

装填条件
|
Column size |
100 X 50 mmI.D. |
|
Packing pressure |
6.5 MPa |
色谱柱性能试验
|
Eluent |
methanol/water(85/15) |
|
Flow rate |
50 mL/min |
| 非常适用于胰岛素等多肽的分离
YMC*GEL/YMC*GEL HG系列有丰富的官能团与不同孔径,可满足大多数客户的制备需求。其中大孔填料非常适于胰岛素等多肽、蛋白质等的分离。同时,由于YMC*GEL HG系列填料与YMC-Pack系列分析色谱柱具有相同的选择性,因此可以轻松实现从分析到制备的规模放大。

|
分析条件 (1), (3) |
|
|
Column |
YMC-Pack C8 (5 µm, 20 nm) 150 X 4.6 mmI.D. |
|
Eluent |
A) water/TFA (100/0.1) B) acetonitrile/TFA (100/0.1) 27%B (0-5 min) 27-40%B (5-20 min) |
|
Flow rate |
0.8 mL/min |
|
Temperature |
ambient |
|
Detection |
UV at 220 nm |
|
分析条件 (2) |
|
|
Column |
YMC*GEL C8 (10 µm, 20 nm) 150 X 50 mmI.D. |
|
Eluent |
A) water/TFA (100/0.1) B) acetonitrile/TFA (100/0.1) 27%B (0-5 min) 27-40%B (5-20 min) |
|
Flow rate |
100 mL/min |
|
Temperature |
ambient |
|
Detection |
UV at 220 nm |
| EPA-EE的制备案例(YMC-Omega)
下图是使用内径为10 mm的色谱柱进行的预备试验,为获取高回收率对流速与载样量进行优化后,放大至内径为200 mm的动态轴向压缩柱,同时将线流速增大至2倍,虽然每次的回收率略有降低,但由于单次运行的时间缩短至原来的一半,因此单位时间内的生产能力为原来的1.8倍,产能因此得到大幅提升。

eicosapentaenoic acid ethyl ester (EPA-EE)

|
Column |
YMC-Omega (10 µm) |
|
Eluent |
甲醇 |
|
Temperature |
ambient |
|
Detection |
UV at 210 nm |
|
Sample |
70% EPA-EE |
| 高分离性能HPLC填料YMC*GEL
|
填料 |
颗粒径 (µm) |
微孔径 (Å) |
产品型号 |
|
ODS-A |
3 |
120 |
AA12S03 |
|
5 |
AA12S05 |
||
|
5 |
300 |
AA30S05 |
|
|
ODS-AM |
3 |
120 |
AM12S03 |
|
5 |
AM12S05 |
||
|
ODS-AQ |
3 |
120 |
AQ12S03 |
|
5 |
AQ12S05 |
||
|
C8 |
5 |
120 |
OC12S05 |
|
300 |
OC30S05 |
||
|
C4 |
5 |
120 |
BU12S05 |
|
300 |
BU30S05 |
||
|
TMS |
5 |
120 |
TM12S05 |
|
Ph (Phenyl) |
5 |
120 |
PH12S05 |
|
CN |
5 |
120 |
CN12S05 |
|
300 |
CN30S05 |
||
|
SIL (Silica) |
5 |
60 |
SL06S05 |
|
120 |
SL12S05 |
||
|
NH2 |
5 |
120 |
NH12S05 |
| 反相HPLC用填料YMC*GEL HG
|
填料 |
颗粒径 (µm) |
微孔径 (Å) |
产品型号 |
|
ODS-A-HG (标准ODS) |
10 |
120 |
AAG12S11 |
|
200 |
AAG20S11 |
||
|
300 |
AAG30S11 |
||
|
15 |
120 |
AAG12S16 |
|
|
200 |
AAG20S16 |
||
|
300 |
AAG30S16 |
||
|
20 |
120 |
AAG12S21 |
|
|
200 |
AAG20S21 |
||
|
300 |
AAG30S21 |
||
|
50 |
120 |
AAG12S50 |
|
|
ODS-AQ-HG (良好分离效果的亲水性化合物) |
10 |
120 |
AQG12S11 |
|
200 |
AQG20S11 |
||
|
300 |
AQG30S11 |
||
|
15 |
120 |
AQG12S16 |
|
|
200 |
AQG20S16 |
||
|
300 |
AQG30S16 |
||
|
20 |
120 |
AQG12S21 |
|
|
200 |
AQG20S21 |
||
|
300 |
AQG30S21 |
||
|
50 |
120 |
AQG12S50 |
|
|
C8-HG |
10 |
120 |
OCG12S11 |
|
200 |
OCG20S11 |
||
|
300 |
OCG30S11 |
||
|
15 |
120 |
OCG12S16 |
|
|
200 |
OCG20S16 |
||
|
300 |
OCG30S16 |
||
|
20 |
120 |
OCG12S21 |
|
|
200 |
OCG20S21 |
||
|
300 |
OCG30S21 |
||
|
50 |
120 |
BUG12S50 |
|
|
C4-HG |
10 |
120 |
BUG12S11 |
|
200 |
BUG20S11 |
||
|
300 |
BUG30S11 |
||
|
15 |
120 |
BUG12S16 |
|
|
200 |
BUG20S16 |
||
|
300 |
BUG30S16 |
||
|
20 |
120 |
BUG12S21 |
|
|
200 |
BUG20S21 |
||
|
300 |
BUG30S21 |
||
|
50 |
120 |
BUG12S50 |
|
|
TMS-HG |
10 |
120 |
TMG12S11 |
|
200 |
TMG20S11 |
||
|
300 |
TMG30S11 |
||
|
15 |
120 |
TMG12S16 |
|
|
200 |
TMG20S16 |
||
|
300 |
TMG30S16 |
||
|
20 |
120 |
TMG12S21 |
|
|
200 |
TMG20S21 |
||
|
300 |
TMG30S21 |
||
|
50 |
120 |
TMG12S50 |
|
|
Ph-HG (Phenyl) |
10 |
120 |
PHG12S11 |
|
200 |
PHG20S11 |
||
|
300 |
PHG30S11 |
||
|
15 |
120 |
PHG12S16 |
|
|
200 |
PHG20S16 |
||
|
300 |
PHG30S16 |
||
|
20 |
120 |
PHG12S21 |
|
|
200 |
PHG20S21 |
||
|
300 |
PHG30S21 |
||
|
50 |
120 |
PHG12S50 |
|
|
CN-HG (Cyano) |
10 |
120 |
CNG12S11 |
|
200 |
CNG20S11 |
||
|
300 |
CNG30S11 |
||
|
15 |
120 |
CNG12S16 |
|
|
200 |
CNG20S16 |
||
|
300 |
CNG30S16 |
||
|
20 |
120 |
CNG12S21 |
|
|
200 |
CNG20S21 |
||
|
300 |
CNG30S21 |
||
|
50 |
120 |
CNG12S50 |
|
|
SIL-HG (Silica) |
10 |
120 |
SLG12S11 |
|
200 |
SLG20S11 |
||
|
300 |
SLG30S11 |
||
|
15 |
120 |
SLG12S16 |
|
|
200 |
SLG20S16 |
||
|
300 |
SLG30S16 |
||
|
20 |
120 |
SLG12S21 |
|
|
200 |
SLG20S21 |
||
|
300 |
SLG30S21 |
||
|
50 |
120 |
SLG12S50 |
|
|
Diol-HG |
10 |
120 |
DLG12S11 |
|
200 |
DLG20S11 |
||
|
300 |
DLG30S11 |
||
|
15 |
120 |
DLG12S16 |
|
|
200 |
DLG20S16 |
||
|
300 |
DLG30S16 |
||
|
20 |
120 |
DLG12S21 |
|
|
200 |
DLG20S21 |
||
|
300 |
DLG30S21 |
||
|
50 |
120 |
DLG12S50 |
|
|
NH2-HG |
10 |
120 |
NHG12S11 |
|
200 |
NHG20S11 |
||
|
300 |
NHG30S11 |
||
|
15 |
120 |
NHG12S16 |
|
|
200 |
NHG20S16 |
||
|
300 |
NHG30S16 |
||
|
20 |
120 |
NHG12S21 |
|
|
200 |
NHG20S21 |
||
|
300 |
NHG30S21 |
||
|
50 |
120 |
NHG12S50 |
| Omega脂肪酸纯化用填料 YMC-Omega
|
填料 |
颗粒径 (µm) |
微孔径 (Å) |
产品型号 |
|
YMC-Omega |
10 |
- |
OMG99S11 |
|
20 |
OMG99S21 |
||
|
50 |
OMG99S50 |
| 快速层析色谱用填料(破碎状填料-颗粒径50 µm)
|
填料 |
产品型号 |
|
SIL |
SLK06I52 |
|
NH2 |
NHK15I52 |
|
Diol |
DLK15I52 |
|
ODS |
ABK15I52 |
|
填料 |
产品型号 |
|
SIL |
SLK06I52 |
|
NH2 |
NHK15I52 |
|
Diol |
DLK15I52 |
|
ODS |
ABK15I52 |
| 快速层析色谱用填料(球形填料-颗粒径25 µm)
|
填料 |
产品型号 |
|
SIL |
SLF08S25 |
|
NH2 |
NHF08S25 |
|
Diol |
DLF08S25 |
|
ODS |
ABF08S25 |
| 开放柱色谱用填料(球形填料)
|
填料 |
颗粒径 (µm) |
孔径 (Å) |
产品型号 |
|
ODS-A |
75 |
60 |
AA06S75 |
|
150 |
AA06SA5 |
||
|
75 |
120 |
AA12S75 |
|
|
150 |
AA12SA5 |
||
|
SIL |
75 |
120 |
SL12S75 |
|
150 |
SL12SA5 |




